MR. BUSH'S CORRESPONDENCE WI H SIR H. HALFORD.

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PREPARATION AND CHARACTERIZATION OF [Ni (MAP) ] ; H- MAP = 2- (METHYLAMINO) PYRIDINE H. Aghabozorg* and H. H. Monfared

We have recently synthesized [Ni (MAP) ] complex [H-MAP= 2- (methylamino) pyridine]. 2- (Methy1amino)pyridine reacts with MeLi in THF and generates the lithium salt (Li-MAP). Further reaction of NiCl with two equivalent of this ligand in THF leads to the formation of a dark red solution. Analytical data, molecular weight, and magnetic susceptibility of this complex confirm the formula [N...

Professor Sir Derek H. R. Barton and Heterocycles

H MR Spectroscopy Outside the Brain

Introduction The majority of clinical applications of H-MR spectroscopy (MRS) concern diseases of the human brain. This is caused by two main reasons: 1) The main clinical reason is that the brain is poorly accessible for biopsies, whereas other organs are more suitable for invasive biopsy investigations. 2) The technical reasons involve lipids, motion and general experience. First, in most org...

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